US3722676A - Ore separation - Google Patents

Ore separation Download PDF

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Publication number
US3722676A
US3722676A US00173776A US3722676DA US3722676A US 3722676 A US3722676 A US 3722676A US 00173776 A US00173776 A US 00173776A US 3722676D A US3722676D A US 3722676DA US 3722676 A US3722676 A US 3722676A
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Prior art keywords
particles
tubes
type
fluid streams
arcuate
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US00173776A
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English (en)
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T Mathews
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Mathews Mining Co
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Mathews Mining Co
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B13/00—Control arrangements specially adapted for wet-separating apparatus or for dressing plant, using physical effects
    • B03B13/02—Control arrangements specially adapted for wet-separating apparatus or for dressing plant, using physical effects using optical effects
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07C—POSTAL SORTING; SORTING INDIVIDUAL ARTICLES, OR BULK MATERIAL FIT TO BE SORTED PIECE-MEAL, e.g. BY PICKING
    • B07C5/00—Sorting according to a characteristic or feature of the articles or material being sorted, e.g. by control effected by devices which detect or measure such characteristic or feature; Sorting by manually actuated devices, e.g. switches
    • B07C5/36—Sorting apparatus characterised by the means used for distribution
    • B07C5/361—Processing or control devices therefor, e.g. escort memory
    • B07C5/362—Separating or distributor mechanisms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07C—POSTAL SORTING; SORTING INDIVIDUAL ARTICLES, OR BULK MATERIAL FIT TO BE SORTED PIECE-MEAL, e.g. BY PICKING
    • B07C5/00—Sorting according to a characteristic or feature of the articles or material being sorted, e.g. by control effected by devices which detect or measure such characteristic or feature; Sorting by manually actuated devices, e.g. switches
    • B07C5/36—Sorting apparatus characterised by the means used for distribution
    • B07C5/363—Sorting apparatus characterised by the means used for distribution by means of air
    • B07C5/367—Sorting apparatus characterised by the means used for distribution by means of air using a plurality of separation means
    • B07C5/368—Sorting apparatus characterised by the means used for distribution by means of air using a plurality of separation means actuated independently

Definitions

  • ABSTRACT There is disclosed herein an apparatus for detecting and separating a desired ore or mineral from a quantity of ore.
  • the apparatus includes a plurality of selectively deflectable flowing fluid streams.
  • the streams are controlled to displace the desired mineral particles from the quantity of ore.
  • Pivotally mounted arcuate tubes normally divert the fluid streams when then are not acting to displace particles, but these tubes are selectively movable to allow the streams to hit desired particles.
  • a screen is used for conveying the ore past the fluid streams in such a manner that the streams may act through the screen to displace the selected particles.
  • Some systems heretofore imployed in making a primary separation of minerals have significant limitations based on mandatory requirements on ore input.
  • One factor constraining such an input is the speed with which the selecting means can separate. This reaction speed affects the volume of material which can be processed in a given time, and is particularly important when small particles or low grade material is to be separated.
  • the reaction time of the system also may reduce the accuracy of selection because the process is less able to initiate and terminate a selection response in an almost instantaneous period of time. With reduced accuracy, the density of'particle input must correspondingly be reduced.
  • the constraint on the density of particles input also reduces the amount of material which can be processed in a given period of time.
  • Another factor which acts as a limitation on the input is the need for an accurate trajectory for the particles passing the selection device.
  • the particles When the particles are allowed to fall past the selection device, their original release should impart a particular velocity to the particles.
  • the particles will then reach the sensor and selection means at a predicted location and time. This is desirable because of the usual reduction in the sensitivity of sensing devices, and the accuracy of separating means, as the distance from the desired particles SUMMARY OF THE INVENTION
  • the present invention involves several novel concepts particularly useful in separations where the desired particles are relatively small.
  • An example, although not intending to be limined thereby, is the separation of diamonds as small as one twenty thousandth inch.
  • the separation of small particles requires the use of a separation device of relatively low mass which can be actuated rapidly, and which can be made sufficiently small so as to separate out the desired particles without also separating out undesired particles.
  • the present concepts accordingly involve means for controlling a flowing fluid stream in a rapid and precise manner.
  • a plurality of arcuate tubes are employed to normally divert a like number of flowing fluid streams away from the particle selection area. These tubes are pivotally mounted so as to greatly reduce theinertia which must be overcome in controlling the fluid streams.
  • an arcuate tube is displaced or moved out of the naturalpath of the flowing stream to allow the stream to impinge upon the particle being selected. In this manner the trajectory ofthe selected particle is changed so that it may be collected in a suitable receptacle.
  • the arcuate tubes can be made relatively small, and actuated rapidly, they allow-short and precise pulses of fluid to impinge upon the desired particles for separation, and function well in separating either wet or dry particles.
  • the concepts of the present invention also include the use of a perforated conveyor in the form of a screen.
  • the slurry preferably is applied to the screen in a layer approximately one particle thick.
  • the screen type belt allows the liquid from the slurry to drain off as the material is conveyed to the detection and separation area.
  • the use of a screen also allows separation of the desired particles through the belt.
  • the - belt conveys the material past sensors which detect the characteristic of the desired particles, such as radiation thereof or radiation from a preferential coating thereon as described in said above patents.
  • the arcuate tubes are mounted under the belt and are actuated in response to the signals from the sensing system to cause liquid to flow through the screen belt and deflect desired particles therefrom into a receptacle.
  • This arrangement eliminates the problems associated with developing a desired trajectory for the particles.
  • the screen arrangement further allows the material tobe introduced in either a wet state or a dry state, and allows the use of a wide range of belt feed speeds.
  • FIG. 1 is a schematic illustration of the separating apparatus according to the present invention showing an arcuate tube in a position to normaliy deflect flowing liquid streams away from the separation area;
  • FIG. 2 is a similar illustration showing an arcuate tube displaced to allow a flowing stream to impinge upon, and thus change the trajectory of, a desired particle;
  • FIG. 3 is a detailed side elevational view of apparatus similar to that of FIGS. 1 and 2 but including a screen type conveyor;
  • FIG. 4 is a partial perspective view of the arrangement of FIG. 3.
  • FIGS. 1 and 2 schematically illustrate apparatus according to the present concepts employing a plurality of pivotally mounted arcuate tubes which are used to normally deflect'a like plurality of continuously flowing liquid streams, but which may be moved or otherwise displaced about a pivot axis to allow one or more streams to impinge upon one or more respective desired particles to be separated.
  • FIGS. 3 and-4 illustrate construction details of this arrangement, and further illustrate its use in conjunction with a moving screen type conveyor or belt wherein the deflecting apparatus is mounted beneath the belt to displace desired particles from the belt rather than accomplishing this operation during free-fall of the particles as schematically illustrated in FIGS. 1 and 2.
  • a sensor 14 is located adjacent the trajectory plane 12 and generates a timed response when a desired or preferred particle passes any one of many discrete areas of observation across the trajectory plane 12 respectively associated with the plural tubes.
  • the sensor response is supplied to one of a bank of double acting actuators 16 which are mechanically linked to pivotally mounted arcuate tubes 18.
  • a typical conveyor belt is 30 to 40 inches wide and, thus, a large plurality of actuators and tubes are employed to select particles falling from any point along the width of the belt; likewise, the sensor 14 includes a like plurality of sensors to completely cover the plane 12 of interest. That is, there is a sensor corresponding to each tube, each sensor observing the area of its respective tube.
  • the actuators 16 serve to pivot respective arcuate tubes 18,to the position shown in FIG. 2 and to return v the tubes to the normal position shown in FIG. 1.
  • FIGS. 1 and 2 a conveyor 10 is shown onto which ore material is applied for feeding the ore into a trajectory plane symbolicallyillustrated by an arrow 12.
  • the latter have a measurable property not possessed by the other material fed to the conveyor. Examples of such property are natural radiation, or fluorescence imparted by minerals to electromagnetic radiation to cause at least a portion thereof to fluorescence at a characteristic wavelength.
  • the latter can be achieved by preferentially coating some of the particles with a tinuous fluid streams are supplied to the inlet ends of the arcuate tubes 18 from a manifold 20 through respective nozzles 22.
  • the arcuate tubes 18 are positioned relative to the streams so that each stream is chanelled through a corresponding arcuate tube 18 onto a deflection plate 24 which diverts the fluid from the system.
  • the ore particles fall along the trajectory plane 12 and into an ore receptacle 26.
  • the sensor 14 observes a particle which is to be separated from the main body of the ore
  • the sensor 14 responds to the observation by triggering the appropriate actuator 16.
  • the actuator pivots its respective arcuate tube 18 for the sensed area away from the continuous fluid stream thereby allowing thestream to directly impinge upon the selected particle, causing the particle to be diverted into the mineral receptacle 28.
  • tubes 18 and nozzles 22 are employed, and the sensor 14 includes a like number of detectors.
  • the arcuate tubes 18 are mounted apart on A; inch centers, and the water jet from eachnozzle 22 is approximately 1/16 inch in diameter.
  • the conveyor belt may be approximately 30 inches wide.
  • the arcuate tube arrangement is particularly advantageous in providing a fast acting deflection system.
  • the arcuate tubes can be made relatively small and light weight so that the same can be moved rapidly by an electromagnetic actuator 16. Furthermore, in the normal position shown in FIG. 1, the .water flow through the arcuate tube 18 tends to maintain the tube I in the fluid-deflecting position as shown, but when the arcuate tube is' partially deflected (rotated counterclockwise as seen in FIGS. 1 and 2) by the actuator 16,
  • the fluid jet on the entry end of the tube from the nozzle 22 and partial amount of fluid remaining toward the outlet end of the tube aids in quickly deflecting the 18 when the entry end of the tube intercepts the fluid stream.
  • FIGS. 3 and 4 there is shown a screen type conveyor 30 and the sensor 14 mounted above the screen, and the actuator assembly mounted beneath the screen for deflecting desired particles therefrom rather than deflecting the particles from the free-fall trajectory 12 upon leaving the conveyor as illustrated in FIG. 1.
  • the sensor 14 may be any of several types of sensors incorporating a plurality of sensing elements across the lateral dimension, or width, of the conveyor for sensing the unique characteristic of desired particles. Exemplary sensing arrangements are disclosed in said aforementioned patents. Suitable sensing devices include electromagnetic radiation sensors, color sensors, reflectivity sensors, radioactivity sensors, thermo-magnetic sensors, and the like. The sensing system employed is principally dictated by the characteristics of the ore to be separated.
  • the sensor 14 includes a row of individual sensing units, as noted above, the number and spacing thereof depending upon the width of the conveyor and the size of the particles to be selected, in order to determine the lateral location of such particles on the screen 30, or in the trajectory plane 12 if the free-fall arrangement of FIGS. 1 and 2 is used. Furthermore, the sensor system 14 includes appropriate electrical circuits for detecting the responses of the respective sensing elements upon detection of a desired particle, and for translating such signals into respective gating signals timed to actuate the selection system at the appropriate instant, and to allow or enable return of the selection system to its normal state following the selection.
  • An exemplary system and sircuits are described and illustrated in said U.S. Pat. No. 3,472,375.
  • the arrangement thereon illustrated describes an exemplary arrangement wherein ore has been treated with a fluorescent material, is irradiated by a radiation source, and the characteristic radiation emitted by desired particles of ore is-detected by an electromagnetic wave sensing means, such as a plurality of photomultiplyers.
  • the sensing or detecting means then provides signals to an amplifier and control circuit which in turn actuates one or more electromagnetic actuators, the particular one or more actuated depends upon the number'and position of desired'particles when were detected.
  • These actuators according to said U.S. Pat; No. 3,472,375, then pivot tubes flexibly coupled with a manifold to supply a stream of fluid for deflecting the desired particle or particles from the nor mal trajectory thereof.
  • arcuate tubes 18 allows a more closely spaced selection apparatus and eliminates the need for flexible connections.
  • These tubes may be operated in any suitable manner, such as by means of electromagnetic actuators of the nature of those illustrated in said U.S. Pat. No. 3,472,375. Any other suitable arrangement may be employed, such as a staggered'arrangement of groups of electromagnetic actuators 34 and 36 mounted approximately 90 apart, each of which is double acting for moving its respective tube in two directions. These actuators are staggered to allow a more compact, or close, spacing of the tubes.
  • the actuators 34 operate the first, third, fifth, etc., tubes and the actuators 36 operate the second,-fourth, sixth, etc., tubes.
  • energization of actuator 34 will pivot the arcuate tube 18 counter-clockwise and thus allow a stream of fluid, such as water, from the nozzle 22 to flow through the screen 30 and impinge upon a particle thereon. Reverse energization of the actuator 34 will return the tube to its normal, fluid deflecting, position.
  • the actuator 36 similarly rotates the next arcuate tube.
  • Any other suitable arrangement for moving the arcuate tubes 18 may be employed, such as a pair of single-acting electromagnetic actuators coupled to each tube, one actuator for moving the tube in one direction and the other actuator for moving the tube in the other direction; a single actuator 34 or 36 for pivoting the tube 18 counter-clockwise and a spring for returning it to its normal position; and the like. The arrangement as illustrated in FIG.
  • Each arcuate tube 18 is secured to a suitable bracket 41 and the linkages 38 and 40 are pivotally coupled with'the brackets for respective pairs of tubes at 42 and 43. That is, the'linkages 38 are connected at the lower ends of the brackets at 42 for the first, third, etc., tubes; whereas, the linkages 40 are connected at the upper ends of the brackets at 43 for the second, third, etc. tubes.
  • Pivot rings 46 are secured to the arcuate tubes 18, and these rings are pivotally mounted on a rod 48. The rings 46 are mounted at a position on the arcuate tubes 18 so as not to interfere with fluid streams from the nozzles 22.
  • the radius of the tubes 18 is selected to sufflciently divert the fluid streams so that the streams will not come in contact with the ore whenthe tube is in a normal, fluid deflecting, position as indicated at FIG. 1 so as to prevent inadvertant selection of worthless material.
  • the stroke of each actuator 34 and 36 is selected to provide sufficient clearence in swinging the upper end of a respective tube 18 from the path of a stream from a nozzle.22 upon. particle selection.
  • the number of arcuate tubes l8' is selected to correspond with the number of sensing elements in the sensor system 14, and is sufficient to cover the width of the selection area. With a 30 inch wide screen, an arrangement for selecting relatively small particles as described previously may include approximately 240 arcuate tubes 18 mounted on inch centers across the width of the screen.
  • a receptacle or collection box 54 is located relatively close to the outer surface of the screen 30, and exand precise positioning thereof are dependent upon the.
  • the trajectory of the material falling from the screen is relatively unpredictable as noted earlier; on the other hand, it is relatively crushed, and put through heavy media separation to derive a material having particle sizes in the range desired.
  • This material is slurred with water to provide a dispersion sufficient to spread on the screen, such as approximately two to five parts of water per one part material, and then is spread on the feed end of the screen belt 30 in a thin layer approximately one particle size thick.
  • the screen has openings of approximately one-twenty thousandth inch, and allows dewatering of the slurry without loss of the material.
  • the screen 30 may be approximately 30 inches wide and be formed of stainless steel thirteen thousandths diameter wire, and
  • the force of gravity on retaining particles on the screen is reduced by approximately 50 to 80 percent. This reduces the force required in deflecting a particle from the outer surface of the screen, while obviating the problems of sensing and deflecting particles freely falling from the screen.
  • the angle of the belt in the separation area also aids in collecting particles in the container 54.
  • the angled portion of the screen may be providedby employing single or plural (so as not to abruptly change the direction of the belt) rollers at upper and lower locations 60 and 61.
  • the screen size or mesh is determined by the minimum particle size desired to be separated.
  • the optimum size isthat which will barely retain the smallest desired particle on the screen. With a coarser screen, the fluid streams are more effective in deflecting particles therefrom.
  • tubes 18 may be mounted on approximately 1s inch centers.
  • the desired material such as diamonds as noted above, are preferentially coated with a fluorescent agent prior to slurrying or as part of the slurry.
  • the sensor 14 is mounted relatively close to the layer of material, and preferably as close as possible inand at a belt speed of 400.feet per minute, approximately 6 feet of belt prior to thedetecting and separating area thereof is sufficient to allow the material to sufficiently drain, unless. the material includes clay which requires a longer draining time.
  • Each arcuate tube 18 may have an inside diameter of approximately 1/16 inch and a radius of approximately 2 inches, with the pivot at. rod 48 falling on a radial line essentially half-way between the ends of the tube.
  • Apparatus for separating first and second solid particles wherein the first type particle has a particular measurable characteristic comprising means for moving the first and 'second particles in a uniform path,
  • sensing means for detecting the measurable charac teristic of the first type particle and for providing control signals
  • nozzle means for forming a plurality of flowing fluid streams
  • plurality of separating means responsive to said signals for allowing selective impingement of the flowing fluid streams on the first type of particle to separate the first type of particles from the second type of particle
  • said plurality of separating means each including an actuator coupled with pivotally mounted arcuate means, said actuator being responsive to a control signal for moving said arcuate means from a normal position to another position for allowing said selective impingement of a flowing fluid stream from a nozzle means on a first type of particle.
  • said means for moving the unseparated ore particles in a uniform path includes perforated conveyor means through which said fluid streams can pass to impinge upon the first type particles.
  • each of said plurality of arcuate means comprises a pivotally mounted arcuate tube, said actuators being actuated by said control signals to rotate each of said tubes independently into and out of the path of a respective flowing fluid stream from said nozzle means.
  • said arcuate means includes a plurality of arcuate tubes pivotally mounted and positioned to normally intercept and deflect the respective flowing fluid streams from said nozzle means, and the actuators coupled with said tubes selectively pivot respective tubes out of the paths of said flowing streams.
  • sensing means extending across the width of said section for detecting the measurable property of the first type of ore particles along said width and providing control signals
  • separating means extending along the width of said section on an opposite side of said section from said sensing means, said separating means being responsive to said signals for causing the flowing fluid streams to flow through said conveyor to provide selective impingement of the flowing fluid streams on the first type of particles to separate the first type of particles from the second type of particles.
  • said separating means comprises a plurality of arcuate tubes through which the fluid streams normally pass and which are selectively pivotable to allow fluid streams to flow through said conveyor.
  • said sensing means is mounted above said separation section and said separating means are mounted below said separation section.
  • said separating means includes a plurality of actuators coupled with a respective plurality of pivotally mounted arcuate tubes, said actuators being responsive to said controlsignals from said sensing means to rotate respective tubes independently into and out of the path of respective flowing fluid streams.
  • said separating means includes a pluralityof pivotally mounted arcuate tubes positioned to normally intercept and deflect the respective flowing fluid streams, and includes actuators coupled with said tubes to selectively pivot respective tubes out of the paths of said flowing streams in response to control signals from said sensing means.

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  • Sorting Of Articles (AREA)
  • Combined Means For Separation Of Solids (AREA)
  • Separation Of Solids By Using Liquids Or Pneumatic Power (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
US00173776A 1971-08-23 1971-08-23 Ore separation Expired - Lifetime US3722676A (en)

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US17377671A 1971-08-23 1971-08-23

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US00173776A Expired - Lifetime US3722676A (en) 1971-08-23 1971-08-23 Ore separation

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US (1) US3722676A (en])
JP (1) JPS5543829B2 (en])
AU (1) AU461223B2 (en])
CA (1) CA955890A (en])
DE (1) DE2241260C3 (en])
FR (1) FR2151349A5 (en])
GB (2) GB1407481A (en])
SE (1) SE380446B (en])
ZA (1) ZA725652B (en])
ZM (1) ZM13572A1 (en])

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4014255A (en) * 1973-12-14 1977-03-29 Coal Industry (Patents) Limited Apparatus for use in determining the character of finely divided or particulate solid material
US4099620A (en) * 1977-03-23 1978-07-11 Acurex Corporation Rejector drive system for sorting apparatus
EP0819247A4 (en) * 1995-04-07 2002-10-23 Tech Resources Pty Ltd METHOD AND DEVICE FOR MATERIAL ANALYSIS
US6753957B1 (en) 2001-08-17 2004-06-22 Florida Institute Of Phosphate Research Mineral detection and content evaluation method
US20120085684A1 (en) * 2009-04-08 2012-04-12 Resteel B.V. Method and Apparatus for Separating a Non-Ferous Metal-Comprising Fraction from Ferrous Scrap
US20140034452A1 (en) * 2010-11-19 2014-02-06 Coldcrete, Inc. Eliminating screens using a perforated wet belt and system and method for cement cooling
CN105618261A (zh) * 2016-03-24 2016-06-01 陈勇 强风吹矿砂式选磁铁矿装置
CN105618253A (zh) * 2016-03-24 2016-06-01 陈勇 一种抛物面击矿砂式选磁铁矿装置
CN110022998A (zh) * 2016-10-28 2019-07-16 美卓（瑞典）公司 探测系统

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS49115955U (en]) * 1973-01-25 1974-10-03
GB8314340D0 (en) * 1983-05-24 1983-06-29 British Petroleum Co Plc Separation technique
JPS61216787A (ja) * 1985-03-19 1986-09-26 株式会社　安西製作所 混入された異物を判定選別して除去をする機構
JPH0324086U (en]) * 1989-07-17 1991-03-13
RU2691418C1 (ru) * 2018-04-09 2019-06-13 Акционерная Компания "АЛРОСА" (публичное акционерное общество) (АК "АЛРОСА" (ПАО)) Способ предконцентрации алмазосодержащих руд

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3472375A (en) * 1967-10-27 1969-10-14 Ted C Mathews Apparatus and method for separating ore

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4014255A (en) * 1973-12-14 1977-03-29 Coal Industry (Patents) Limited Apparatus for use in determining the character of finely divided or particulate solid material
US4099620A (en) * 1977-03-23 1978-07-11 Acurex Corporation Rejector drive system for sorting apparatus
EP0819247A4 (en) * 1995-04-07 2002-10-23 Tech Resources Pty Ltd METHOD AND DEVICE FOR MATERIAL ANALYSIS
US6753957B1 (en) 2001-08-17 2004-06-22 Florida Institute Of Phosphate Research Mineral detection and content evaluation method
US20120085684A1 (en) * 2009-04-08 2012-04-12 Resteel B.V. Method and Apparatus for Separating a Non-Ferous Metal-Comprising Fraction from Ferrous Scrap
US20140034452A1 (en) * 2010-11-19 2014-02-06 Coldcrete, Inc. Eliminating screens using a perforated wet belt and system and method for cement cooling
CN105618261A (zh) * 2016-03-24 2016-06-01 陈勇 强风吹矿砂式选磁铁矿装置
CN105618253A (zh) * 2016-03-24 2016-06-01 陈勇 一种抛物面击矿砂式选磁铁矿装置
CN110022998A (zh) * 2016-10-28 2019-07-16 美卓（瑞典）公司 探测系统
CN110022998B (zh) * 2016-10-28 2021-06-01 美卓（瑞典）公司 探测系统
US11224897B2 (en) * 2016-10-28 2022-01-18 Metso Sweden Ab Detection system
US11731166B2 (en) 2016-10-28 2023-08-22 Metso Sweden Ab Detection system

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AU461223B2 (en) 1975-05-22
CA955890A (en) 1974-10-08
ZA725652B (en) 1973-04-25
DE2241260C3 (de) 1981-12-17
GB1407481A (en) 1975-09-24
FR2151349A5 (en]) 1973-04-13
ZM13572A1 (en) 1973-06-21
AU4570172A (en) 1974-02-21
DE2241260A1 (de) 1973-03-01
GB1407482A (en) 1975-09-24
SE380446B (sv) 1975-11-10
JPS5543829B2 (en]) 1980-11-08
JPS4834703A (en]) 1973-05-22
DE2241260B2 (de) 1981-02-26

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